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Polymer Crystallization II: From Chain Microstructure to Processing
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Extra resources for Polymer Crystallization II: From Chain Microstructure to Processing
Sample text
22. Quenched and aged samples are shown with solid and dashed lines, respectively. Adapted with permission from [153] Form II, as revealed by the presence of the indicated diagnostic (200)II, (220)II and (213)II + (311)II reflections [95, 177]. On the other hand, the solid-state transformation to the trigonal Form I is practically completed after 1 month of storage at room temperature, as evidenced by the characteristic diffraction peaks of the (110)I, (300)I and (220)I + (211)I planes of Form I.
This peculiar temperature dependence in i-PP deserves further experimental investigation. 5 Overlooked Examples of Cross-Nucleation in Semicrystalline Polymers Although not necessarily discussed in these terms, the peculiar spherulitic morphology arising from cross-nucleation/growth transition has been observed in a few other polymers, namely in low molecular weight PHP and PBA [74, 77]. Short chains of PHP are able to arrange themselves in the δ-phase, with helical conformation, or in the all-trans β- and γ-polymorphs (see Sect.
At TC1, concomitant crystallization of β- and α-spherulites occurs. Figure 12a shows the morphology developed at TC2. The cores of the two spherulites, indicated in red in the image, are the α- and β-crystals grown at TC1. The parts highlighted with green symbols are those formed at TC2. Because TC2 lies above Tβα, the growth of the β-spherulite (Fig. 12a, left side) is frequently interrupted by β-to-α growth transitions. On the other hand, the α-phase spherulite (Fig. 12a, right side) continues growth in the monoclinic (α-) modification.