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Extra info for Polymer Crystallization I: From Chain Microstructure to Processing
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References . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 46 53 59 73 84 85 1 Introduction The uniaxial deformation of semicrystalline polymers having spherulitic or lamellar morphology transforms an initially isotropic material into oriented fibers. In semicrystalline polymers, the complex interwoven structure of amorphous and crystalline phases that are tightly intermingled [1] entails that the deformation process is complex [2, 3, 4, 5–9].
17. With an increase in comonomer content, the morphology of polymer crystals decays from lamella to granular crystallites. Because the crystallizable bonds are almost completely used by the crystallites at low temperatures, polymer chains trespass several crystallites to make a network in 3D space. In this sense, the crystallites act as physical crosslinking points, which enables homogeneous LLDPE samples with high enough comonomer content to perform as thermoplastic elastomers [70]. In ethylene-based homogeneous copolymers, relatively small comonomers such as propylene residues still have the possibility of entering the crystalline region of ethylene sequences [50].
26 are data for HPBDs that are models for random ethylene–1-butene (EB) copolymers. 2 mol% and molar masses ranging from 800 to 420,000 g/mol were studied [96]. These samples were first cooled from 200 C to 40 C at a rate of 10 C/min to develop a standard crystalline state. Then, the samples were heated to different annealing temperatures (Tmelt) for 5 min. The second-round crystallization temperatures (Tc_peak) on DSC cooling curves were compared to test for the memory effect of crystallization (see Fig.